编号:FTJS05693
篇名:绿色可磁性分离二氧化硅包裹镍铁尖晶石负载硫酸氢铁纳米粒子催化剂用于合成1,8-二氧十氢吖啶合成(英文)
作者:Amir Khojastehnezhad; Mohammad Rahimizadeh; Hossein Eshghi;
关键词:Magnetically separable catalyst; Ferric hydrogen sulfate; Nickel ferrite nanoparticles; 1,8-Dioxodec
机构: Department of Chemistry,Faculty of Sciences,Ferdowsi University of Mashhad; Department of Chemistry,
摘要: A new magnetically separable catalyst consisting of ferric hydrogen sulfate supported on silica-coated nickel ferrite nanoparticles was prepared.The synthesized catalyst was characterized using vibrating sample magnetometry,X-ray diffraction,transmission electron microscopy,scanning electron microscopy,and Fourier transform infrared spectroscopy.This new magnetic catalyst was shown to be an efficient heterogeneous catalyst for the synthesis of 1,8- dioxodecahydroacridines under solvent-free conditions.The catalyst is readily recovered by simple magnetic decantation and can be recycled several times with no significant loss of catalytic activity.